Operando scanning electrochemical probe microscopy during electrocatalysis

C Santana Santos, BN Jaato, I Sanjuán… - Chemical …, 2023 - ACS Publications
Scanning electrochemical probe microscopy (SEPM) techniques can disclose the local
electrochemical reactivity of interfaces in single-entity and sub-entity studies. Operando …

Scanning electrochemical microscopy: a comprehensive review of experimental parameters from 1989 to 2015

D Polcari, P Dauphin-Ducharme, J Mauzeroll - Chemical reviews, 2016 - ACS Publications
Scanning electrochemical microscopy (SECM) is an electroanalytical scanning probe
technique capable of imaging substrate topography and local reactivity with high resolution …

Scanning electrochemical microscopy

FRF Fan, B Liu, J Mauzeroll - Handbook of electrochemistry, 2007 - Elsevier
Publisher Summary The chapter discusses various techniques and applications of scanning
electrochemical microscopy (SECM), one of the scanning probe microscopies (SPM) in …

Electrocatalytic activity and stability of nitrogen-containing carbon nanotubes in the oxygen reduction reaction

S Kundu, TC Nagaiah, W Xia, Y Wang… - The Journal of …, 2009 - ACS Publications
Nitrogen-containing carbon nanotubes (NCNTs) were prepared via pyrolysis of acetonitrile
over cobalt catalysts at different temperatures to control the nitrogen content. The changes in …

Scanning electrochemical microscopy

S Amemiya, AJ Bard, FRF Fan, MV Mirkin… - Annu. Rev. Anal …, 2008 - annualreviews.org
This review describes work done in scanning electrochemical microscopy (SECM) since
2000 with an emphasis on new applications and important trends, such as nanometer-sized …

Nanoelectrodes: Applications in electrocatalysis, single-cell analysis and high-resolution electrochemical imaging

J Clausmeyer, W Schuhmann - TrAC Trends in Analytical Chemistry, 2016 - Elsevier
High sensitivity and high spatial resolution in localized electrochemical measurements are
the key advantages of electroanalysis using nanometer-sized electrodes. Due to recent …

Atomic force microscopy-Scanning electrochemical microscopy (AFM-SECM) for nanoscale topographical and electrochemical characterization: Principles …

X Shi, W Qing, T Marhaba, W Zhang - Electrochimica Acta, 2020 - Elsevier
Abstract Atomic Force Microscopy-Scanning Electrochemical Microscopy (AFM-SECM) has
evolved to be a powerful tool for simultaneous topographical-electrochemical …

Fluorescence coupling for direct imaging of electrocatalytic heterogeneity

JP Guerrette, SJ Percival, B Zhang - Journal of the American …, 2013 - ACS Publications
Here we report the use of fluorescence microscopy and closed bipolar electrodes to reveal
electrochemical and electrocatalytic activity on large electrochemical arrays. We …

[HTML][HTML] Investigating local corrosion processes of magnesium alloys with scanning probe electrochemical techniques: A review

MCL de Oliveira, RMP da Silva, RM Souto… - Journal of Magnesium …, 2022 - Elsevier
The study of corrosion of magnesium and its alloys has emerged a hot topic in the
applications of lightweight structural materials. The inherently high electrochemical activity of …

In situ electrochemical mapping of lithium–sulfur battery interfaces using AFM–SECM

K Mahankali, NK Thangavel, LM Reddy Arava - Nano Letters, 2019 - ACS Publications
Although lithium–sulfur (Li–S) batteries are explored extensively, several features of the
lithium polysulfides (LiPS) redox mechanism at the electrode/electrolyte interface still remain …