Developments in the Karplus equation as they relate to the NMR coupling constants of carbohydrates

B Coxon - Advances in carbohydrate chemistry and biochemistry, 2009 - Elsevier
The development of Karplus‐type formulas that relate the NMR coupling constants of
carbohydrates and related ma olecules to the dihedral angle between the coupled nuclei is …

Long-range proton–carbon coupling constants: NMR methods and applications

T Parella, JF Espinosa - Progress in Nuclear Magnetic Resonance …, 2013 - Elsevier
A general review of novel NMR methods to measure heteronuclear long-range proton–
carbon coupling constants (n J CH; n> 1) in small molecules is made. NMR experiments are …

The CLIP/CLAP-HSQC: pure absorptive spectra for the measurement of one-bond couplings

A Enthart, JC Freudenberger, J Furrer, H Kessler… - Journal of Magnetic …, 2008 - Elsevier
Heteronuclear residual dipolar one-bond couplings of organic molecules at natural
abundance are most easily measured using t2 coupled HSQC spectra. However, inevitably …

Identification and quantification of flavonoids and ellagic acid derivatives in therapeutically important Drosera species by LC–DAD, LC–NMR, NMR, and LC–MS

M Zehl, C Braunberger, J Conrad, M Crnogorac… - Analytical and …, 2011 - Springer
Droserae herba is a drug commonly used for treatment of convulsive or whooping cough
since the seventeenth century. Because of the contribution of flavonoids and ellagic acid …

Pure In‐Phase Heteronuclear Correlation NMR Experiments

L Castañar, J Saurí, RT Williamson, A Virgili… - Angewandte …, 2014 - Wiley Online Library
A general NMR approach to provide pure in‐phase (PIP) multiplets in heteronuclear
correlation experiments is described. The implementation of a zero‐quantum filter efficiently …

LC–NMR, NMR, and LC–MS identification and LC–DAD quantification of flavonoids and ellagic acid derivatives in Drosera peltata

C Braunberger, M Zehl, J Conrad, S Fischer… - … of Chromatography B, 2013 - Elsevier
The herb of Drosera peltata, commonly named the shield sundew, is used as an antitussive
in phytotherapy, although the plants' composition has not been determined in detail so far …

PE HSQC: A simple experiment for simultaneous and sign-sensitive measurement of (1JCH+ DCH) and (2JHH+ DHH) couplings

P Tzvetkova, S Simova, B Luy - Journal of Magnetic Resonance, 2007 - Elsevier
The angular information content of residual dipolar couplings between nuclei of fixed
distance makes the accurate and sign-sensitive measurement of (1JCH+ DCH) and (2JHH+ …

Pure shift edited NMR methodologies for the extraction of Homo-and heteronuclear couplings with ultra-high resolution

SK Mishra, N Suryaprakash - Progress in Nuclear Magnetic Resonance …, 2023 - Elsevier
The scalar couplings that result in the splitting of the signals in the NMR spectrum arise due
to the interaction of the nuclear spins, whereby the spin polarization is transmitted through …

29Si NMR in solid state with CPMG acquisition under MAS

JW Wiench, VSY Lin, M Pruski - Journal of Magnetic Resonance, 2008 - Elsevier
A remarkable enhancement of sensitivity can be often achieved in 29Si solid-state NMR by
applying the well-known Carr–Purcell–Meiboom–Gill (CPMG) train of rotor-synchronized π …

Quantitative two-dimensional HSQC experiment for high magnetic field NMR spectrometers

H Koskela, O Heikkilä, I Kilpeläinen… - Journal of Magnetic …, 2010 - Elsevier
The finite RF power available on carbon channel in proton–carbon correlation experiments
leads to non-uniform cross peak intensity response across carbon chemical shift range …