[HTML][HTML] High-resolution 1H NMR of powdered solids by homonuclear dipolar decoupling
FM Paruzzo, L Emsley - Journal of Magnetic Resonance, 2019 - Elsevier
The development of homonuclear dipolar decoupling sequences to obtain high-resolution 1
H NMR spectra from solids has recently celebrated its 50th birthday. Over the years, a series …
H NMR spectra from solids has recently celebrated its 50th birthday. Over the years, a series …
New insights into the use of hydroxypropyl cellulose for drug solubility enhancement: An analytical study of sub‐molecular interactions with fenofibrate in solid state …
M Martin‐Pastor, E Stoyanov - Journal of Polymer Science, 2021 - Wiley Online Library
Hydroxypropyl cellulose (HPC) is a solubility enhancer used for poorly soluble drugs, nano‐
suspensions and amorphous solid dispersions (ASD). However, the underlying mechanism …
suspensions and amorphous solid dispersions (ASD). However, the underlying mechanism …
Crystal structure validation of verinurad via proton-detected ultra-fast MAS NMR and machine learning
D Torodii, JB Holmes, P Moutzouri, SON Lill… - Faraday …, 2024 - pubs.rsc.org
The recent development of ultra-fast magic-angle spinning (MAS)(> 100 kHz) provides new
opportunities for structural characterization in solids. Here, we use NMR crystallography to …
opportunities for structural characterization in solids. Here, we use NMR crystallography to …
[HTML][HTML] Origin of the residual line width under frequency-switched Lee–Goldburg decoupling in MAS solid-state NMR
J Hellwagner, L Grunwald, M Ochsner… - Magnetic …, 2020 - mr.copernicus.org
Homonuclear decoupling sequences in solid-state nuclear magnetic resonance (NMR)
under magic-angle spinning (MAS) show experimentally significantly larger residual line …
under magic-angle spinning (MAS) show experimentally significantly larger residual line …
[HTML][HTML] Echo modulations under homonuclear decoupling
K Aebischer, M Ernst - Journal of Magnetic Resonance, 2023 - Elsevier
A simple Hahn echo in a single-spin system with a static Hamiltonian can lead to echo
modulations if the static Hamiltonian contains a component along the direction of the echo …
modulations if the static Hamiltonian contains a component along the direction of the echo …
Residual proton line width under refocused frequency-switched Lee-Goldburg decoupling in MAS NMR
K Aebischer, M Ernst - Physical Chemistry Chemical Physics, 2023 - pubs.rsc.org
Despite many decades of research, homonuclear decoupling in solid-state NMR under
magic-angle spinning (MAS) has yet to reach a point where the achievable proton line …
magic-angle spinning (MAS) has yet to reach a point where the achievable proton line …
The Design of Experimentally Robust Pulse Sequences in Solid-State NMR
J Hellwagner - 2019 - research-collection.ethz.ch
Solid-state NMR is a powerful tool for the study of the structural and dynamic properties of
materials and biomolecules. The strength of solid-state NMR lies in the ability to coherently …
materials and biomolecules. The strength of solid-state NMR lies in the ability to coherently …