Solid state NMR for nonexperts: an overview of simple but general practical methods

IG Shenderovich, HH Limbach - Solids, 2021 - mdpi.com
There are varieties of methods available for the exploration of solids using nuclear magnetic
resonance (NMR) spectroscopy. Some of these methods are quite sophisticated, others …

Additives in halide perovskite for blue-light-emitting diodes: passivating agents or crystallization modulators?

NF Jamaludin, N Yantara, B Febriansyah… - ACS Energy …, 2021 - ACS Publications
Successful adoption of defect management and carrier confinement strategies in
Ruddlesden–Popper (RP) perovskites has driven the impressive improvements to …

P O Moiety as an Ambidextrous Hydrogen Bond Acceptor

EY Tupikina, M Bodensteiner, PM Tolstoy… - The Journal of …, 2018 - ACS Publications
Hydrogen bond patterns of crystals of phosphinic, phosphonic, and phosphoric acids and
their cocrystals with phosphine oxides were studied using 31P NMR and single-crystal X-ray …

Actual symmetry of symmetric molecular adducts in the gas phase, solution and in the solid state

IG Shenderovich - Symmetry, 2021 - mdpi.com
This review discusses molecular adducts, whose composition allows a symmetric structure.
Such adducts are popular model systems, as they are useful for analyzing the effect of …

Immobilized di (hydroperoxy) propane adducts of phosphine oxides as traceless and recyclable oxidizing agents

JC Hoefler, A Vu, AJ Perez, J Blümel - Applied Surface Science, 2023 - Elsevier
Oxidations represent important reactions that are ubiquitous in academia and industry.
Hydrogen peroxide (H 2 O 2) is a common source of active oxygen for oxidations. H 2 O 2 is …

Hydrogen peroxide adducts of triarylphosphine oxides

FF Arp, N Bhuvanesh, J Blümel - Dalton Transactions, 2019 - pubs.rsc.org
Five new hydrogen peroxide adducts of phosphine oxides (p-Tol3PO· H2O2) 2 (1),(o-
Tol3PO· H2O2) 2 (2),(o-Tol2PhPO· H2O2) 2 (3),(p-Tol3PO) 2· H2O2 (4), and (o-TolPh2PO) …

Probing the Brønsted Acidity of the External Surface of Faujasite‐Type Zeolites

L Lakiss, A Vicente, JP Gilson, V Valtchev… - …, 2020 - Wiley Online Library
We outline two methodologies to selectively characterize the Brønsted acidity of the external
surface of FAU‐type zeolites by IR and NMR spectroscopy of adsorbed basic probe …

Cyclic trimers of phosphinic acids in polar aprotic solvent: symmetry, chirality and H/D isotope effects on NMR chemical shifts

VV Mulloyarova, IS Giba, MA Kostin… - Physical Chemistry …, 2018 - pubs.rsc.org
The hydrogen-bonded self-associates of dimethylphosphinic (1), diphenylphosphoric (2),
phenylphosphinic (3), and bis (2, 4, 4-trimethylpentyl) phosphinic (4) acids have been …

For whom a puddle is the sea? Adsorption of organic guests on hydrated MCM-41 silica

IG Shenderovich - Langmuir, 2020 - ACS Publications
Thermal and hydration effects on the mobility of compact and branched organic molecules
and a bulky pharmaceutical substance loaded in submonolayer amounts onto mesoporous …

A DFT Protocol for the Prediction of 31P NMR Chemical Shifts of Phosphine Ligands in First-Row Transition-Metal Complexes

PA Payard, LA Perego, L Grimaud, I Ciofini - Organometallics, 2020 - ACS Publications
While 31P NMR is a major technique to characterize phosphine-ligated transition-metal
complexes—which are ubiquitous in catalysis—31P NMR chemical shifts are difficult to …