X-ray diffraction: A powerful technique for the multiple-length-scale structural analysis of nanomaterials

C Giannini, M Ladisa, D Altamura, D Siliqi, T Sibillano… - Crystals, 2016 - mdpi.com
During recent decades innovative nanomaterials have been extensively studied, aiming at
both investigating the structure-property relationship and discovering new properties, in …

Pair distribution functions from neutron total scattering for the study of local structure in disordered materials

MT Dove, G Li - Nuclear Analysis, 2022 - Elsevier
With the development of pulsed spallation sources of neutrons in recent years has come the
possibility to generate intense beams of higher energy than possible at reactor sources. This …

Quick and robust PDF data acquisition using a laboratory single-crystal X-ray diffractometer for study of polynuclear lanthanide complexes in solid form and in solution

D Tsymbarenko, D Grebenyuk… - Journal of Applied …, 2022 - journals.iucr.org
Self-assembled polynuclear lanthanide hydroxo complexes are important objects in the
reticular chemistry approach to the design of various functional materials. Revealing their …

Pushing data quality for laboratory pair distribution function experiments

SLJ Thomae, N Prinz, T Hartmann, M Teck… - Review of Scientific …, 2019 - pubs.aip.org
Over the last decade, some studies with laboratory pair distribution function (PDF) data
emerged. Yet, limited Q max or instrumental resolution impeded in-depth structural …

Nanostructure and pore size control of template-free synthesised mesoporous magnesium carbonate

O Cheung, P Zhang, S Frykstrand, H Zheng, T Yang… - RSC …, 2016 - pubs.rsc.org
The structure of mesoporous magnesium carbonate (MMC) first presented in 2013 is
investigated using a bottom-up approach. MMC is found to be built from the aggregation of …

[PDF][PDF] Symmetry-adapted pair distribution function analysis (SAPA): a novel approach to evaluating lattice dynamics and local distortions from total scattering data

TA Bird, A Herlihy, MS Senn - Journal of Applied Crystallography, 2021 - journals.iucr.org
A novel symmetry-adapted pair distribution function analysis (SAPA) method for extracting
information on local distortions from pair distribution function data is introduced. The …

[HTML][HTML] High-performance small-and wide-angle X-ray scattering (SAXS/WAXS) experiments on a multi-functional laboratory goniometer platform with easily …

J Bolze, V Kogan, D Beckers, M Fransen - Review of Scientific …, 2018 - pubs.aip.org
Small-angle X-ray scattering (SAXS) is a well-established, versatile technique for the
analysis of nanoscale structures and dimensions, eg, in liquid dispersions, thin solid objects …

[HTML][HTML] Highly versatile laboratory X-ray scattering instrument enabling (nano-) material structure analysis on multiple length scales by covering a scattering vector …

J Bolze, M Gateshki - Review of Scientific Instruments, 2019 - pubs.aip.org
A compact laboratory X-ray scattering platform that uniquely enables for high-performance
ultra-small-angle X-ray scattering (USAXS), small-and wide-angle X-ray scattering …

Data quality in laboratory convergent-beam X-ray total scattering

PC Metz, MR Koehler, K Page - Applied Crystallography, 2024 - journals.iucr.org
Measurement of laboratory atomic pair distribution function data has improved with
contemporary X-ray sources, optics and detectors, with acquisition times of the order of …

Structural Study of Nano-Sized Gahnite (ZnAl2O4): From the Average to the Local Scale

G Confalonieri, N Rotiroti, A Bernasconi, M Dapiaggi - Nanomaterials, 2020 - mdpi.com
Spinel gahnite (ZnAl2O4) has been obtained through a hydrothermal synthesis method with
a grain size of about 2 nm. The sample was calcined for a few hours at two different …