Recent advances in petroleum analysis by mass spectrometry

E Niyonsaba, JM Manheim, R Yerabolu… - Analytical …, 2018 - ACS Publications
Chemical characterization of petroleum is a challenging task due to its inherently complex
nature. For example, crude oil is believed to have as many or more compounds than the …

Sample preparation methods for subsequent determination of metals and non-metals in crude oil—A review

PA Mello, JSF Pereira, MF Mesko, JS Barin… - Analytica chimica …, 2012 - Elsevier
In this review sample preparation strategies used for crude oil digestion in last ten years are
discussed focusing on further metals and non-metals determination. One of the main …

21 tesla FT-ICR mass spectrometer for ultrahigh-resolution analysis of complex organic mixtures

DF Smith, DC Podgorski, RP Rodgers… - Analytical …, 2018 - ACS Publications
We describe complex organic mixture analysis by 21 tesla (T) Fourier transform ion cyclotron
resonance mass spectrometry (FT-ICR MS). Ultrahigh mass-resolving power (m/Δ m 50%> 2 …

Water-in-crude oil emulsion stabilization: review and unanswered questions

PK Kilpatrick - Energy & Fuels, 2012 - ACS Publications
Emulsions of oil droplets in water but more typically water droplets in oil are common in the
production, transportation, and refining of petroleum and related products. Emulsions of …

21 Tesla Fourier transform ion cyclotron resonance mass spectrometer: a national resource for ultrahigh resolution mass analysis

CL Hendrickson, JP Quinn, NK Kaiser… - Journal of the …, 2015 - ACS Publications
We describe the design and initial performance of the first 21 tesla Fourier transform ion
cyclotron resonance (FT-ICR) mass spectrometer. The 21 tesla magnet is the highest field …

High resolution mass spectrometry

F Xian, CL Hendrickson, AG Marshall - Analytical chemistry, 2012 - ACS Publications
This review focuses on recent advances in instrumentation, techniques, and applications of
the highest resolution mass analyzers (multipass time of flight (TOF), orbitrap, and Fourier …

Review of analytical strategies in the production and upgrading of bio-oils derived from lignocellulosic biomass

PK Kanaujia, YK Sharma, MO Garg, D Tripathi… - Journal of Analytical and …, 2014 - Elsevier
Lignocellulosic biomass is a promising source of renewable energy and valuable chemicals.
It is abundant in several forms which may be pyrolyzed to give gases, condensates and …

Heavy petroleum composition. 3. Asphaltene aggregation

AM McKenna, LJ Donald, JE Fitzsimmons, P Juyal… - Energy & …, 2013 - ACS Publications
Molecular characterization of asphaltenes by conventional analytical techniques is a
challenge because of their compositional complexity, high heteroatom content, and …

Heavy petroleum composition. 4. Asphaltene compositional space

AM McKenna, AG Marshall, RP Rodgers - Energy & Fuels, 2013 - ACS Publications
Asphaltenes and maltenes are defined operationally by solubility (in, eg, heptane).
Asphaltenes self-associate in solution and form putative nanoaggregates composed of …

Expansion of the analytical window for oil spill characterization by ultrahigh resolution mass spectrometry: beyond gas chromatography

AM McKenna, RK Nelson, CM Reddy… - … science & technology, 2013 - ACS Publications
Traditional tools for routine environmental analysis and forensic chemistry of petroleum have
relied almost exclusively on gas chromatography–mass spectrometry (GC-MS), although …