Solid-state NMR: Methods for biological solids
S Ahlawat, KR Mote, NA Lakomek… - Chemical Reviews, 2022 - ACS Publications
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …
transformed from a spectroscopic technique investigating small molecules and industrial …
Solid-state NMR dipolar and chemical shift anisotropy recoupling techniques for structural and dynamical studies in biological systems
With the development of NMR methodology and technology during the past decades, solid-
state NMR (ssNMR) has become a particularly important tool for investigating structure and …
state NMR (ssNMR) has become a particularly important tool for investigating structure and …
SIMPSON: a general simulation program for solid-state NMR spectroscopy
M Bak, JT Rasmussen, NC Nielsen - Journal of magnetic resonance, 2011 - Elsevier
A computer program for fast and accurate numerical simulation of solid-state NMR
experiments is described. The program is designed to emulate a NMR spectrometer by …
experiments is described. The program is designed to emulate a NMR spectrometer by …
Experimental constraints on quaternary structure in Alzheimer's β-amyloid fibrils
AT Petkova, WM Yau, R Tycko - Biochemistry, 2006 - ACS Publications
We describe solid-state nuclear magnetic resonance (NMR) measurements on fibrils formed
by the 40-residue β-amyloid peptide associated with Alzheimer's disease (Aβ1-40) that …
by the 40-residue β-amyloid peptide associated with Alzheimer's disease (Aβ1-40) that …
Cross polarization in the tilted frame: assignment and spectral simplification in heteronuclear spin systems
A frequency selective heteronuclear polarization transfer technique is introduced for rotating
solids. In this method, radiofrequency fields comparable with the frequency offsets are …
solids. In this method, radiofrequency fields comparable with the frequency offsets are …
Amyloid Fibril Formation by Aβ16-22, a Seven-Residue Fragment of the Alzheimer's β-Amyloid Peptide, and Structural Characterization by Solid State NMR
JJ Balbach, Y Ishii, ON Antzutkin, RD Leapman… - Biochemistry, 2000 - ACS Publications
The seven-residue peptide N-acetyl-Lys-Leu-Val-Phe-Phe-Ala-Glu-NH2, called Aβ16-22
and representing residues 16− 22 of the full-length β-amyloid peptide associated with …
and representing residues 16− 22 of the full-length β-amyloid peptide associated with …
Chemical shift correlation spectroscopy in rotating solids: Radio frequency‐driven dipolar recoupling and longitudinal exchange
AE Bennett, RG Griffin, JH Ok, S Vega - The Journal of chemical …, 1992 - pubs.aip.org
In powdered solids, the methods of magic angle spinning (MAS), 1-4 proton decoupling, and
cross polarizationS are now accepted as standard procedures for observing high resolution …
cross polarizationS are now accepted as standard procedures for observing high resolution …
Broadband dipolar recoupling in the nuclear magnetic resonance of rotating solids: A compensated C7 pulse sequence
We introduce an improved variant of the C7 pulse-sequence for efficient recoupling of spin-
1/2 pair dipolar interactions in magic-angle spinning solid-state NMR spectroscopy. The …
1/2 pair dipolar interactions in magic-angle spinning solid-state NMR spectroscopy. The …
Solid‐state NMR spectroscopic methods in chemistry
DD Laws, HML Bitter, A Jerschow - Angewandte Chemie …, 2002 - Wiley Online Library
Over the last decades, NMR spectroscopy has grown into an indispensable tool for chemical
analysis, structure determination, and the study of dynamics in organic, inorganic, and …
analysis, structure determination, and the study of dynamics in organic, inorganic, and …
Through-bond carbon− carbon connectivities in disordered solids by NMR
Using a refocused INADEQUATE NMR experiment we show that homonuclear carbon−
carbon through-bond correlations can be obtained in disordered organic solids where the …
carbon through-bond correlations can be obtained in disordered organic solids where the …