Setting multivariate and correlated acceptance limits for assessing the conformity of items

RJN Bettencourt da Silva, F Lourenço… - Analytical Letters, 2022 - Taylor & Francis
Many industrial products, foodstuffs and environmental samples are checked for values of
different chemical parameters against tolerance limits or intervals defined in a specification …

Risk assessment in monitoring of water analysis of a Brazilian river

LP Brandão, VF Silva, M Bassi, EC de Oliveira - Molecules, 2022 - mdpi.com
This study aimed to introduce non-parametric tests and guard bands to assess the
compliance of some river water properties with Brazilian environmental regulations. Due to …

[HTML][HTML] Risk of false conformity assessment applied to automotive fuel analysis: A multiparameter approach

EC de Oliveira, FR Lourenço - Chemosphere, 2021 - Elsevier
The low-quality of automotive fuels may lead to the generation of pollutants harmful to both
environmental and human health. The quality evaluation of automotive fuels requires a …

Risk of false conformity decisions of multicomponent items controlled by correlated measurement results due to the sharing of analytical steps

FR Lourenco, RJNB da Silva - Talanta, 2019 - Elsevier
The assessment of the conformity of some items, such as medicines, food products or
drinking waters, with limits set for several of their components, involves the determination of …

IUPAC/CITAC Guide: Evaluation of risks of false decisions in conformity assessment of a multicomponent material or object due to measurement uncertainty (IUPAC …

I Kuselman, FR Pennecchi, RJNB da Silva… - Pure and Applied …, 2021 - degruyter.com
Risks of a false decision on conformity of the chemical composition of a multicomponent
material or object due to measurement uncertainty are defined using the Bayesian …

Spreadsheet for evaluation of global risks in conformity assessment of a multicomponent material or object

RJNB da Silva, FR Lourenço, FR Pennecchi… - Chemometrics and …, 2019 - Elsevier
A user-friendly MS-Excel spreadsheet is developed for evaluation of global consumer's and
producer's risks in conformity assessment of chemical composition of a multicomponent …

Measurement uncertainty arising from sampling and analytical steps of dissolution test of prednisone tablets

AY Sano, FR Lourenço - Journal of Pharmaceutical and Biomedical …, 2023 - Elsevier
Dissolution is used to determine the rate and extent of drug release from the dosage form
into a dissolution medium, which allow to assess the batch-to-batch variability. Considering …

Evaluation of seawater composition in a vast area from the Monte Carlo simulation of georeferenced information in a Bayesian framework

C Borges, C Palma, T Dadamos, RJNB da Silva - Chemosphere, 2021 - Elsevier
The detection of composition or pollution trends of vast environmental water areas, from a
river, lake or sea, requires the determination of the mean concentration of the studied …

Improved spreadsheet method for determination of between components metrological correlation due to the sharing of analytical steps

L Separovic, RJNB da Silva, FR Lourenco - Chemometrics and Intelligent …, 2019 - Elsevier
Every multi-parameter conformity assessment presents some risk due to measurement
uncertainty, that may be increased or decreased when data are correlated. Correlation may …

Frequentist approach for estimation of false decision risks in conformity assessment based on measurement uncertainty of liquid chromatography analytical …

L Separovic, FR Lourenço - Journal of Pharmaceutical and Biomedical …, 2020 - Elsevier
The measurement uncertainty (MU) related to analytical results can lead to false decisions in
conformity assessment, such as accepting or rejecting incorrectly a medicine lot (consumer's …