Solid-state NMR spectroscopy

B Reif, SE Ashbrook, L Emsley, M Hong - Nature Reviews Methods …, 2021 - nature.com
Solid-state nuclear magnetic resonance (NMR) spectroscopy is an atomic-level method to
determine the chemical structure, 3D structure and dynamics of solids and semi-solids. This …

Applications of high-resolution 1H solid-state NMR

SP Brown - Solid State Nuclear Magnetic Resonance, 2012 - Elsevier
This article reviews the large increase in applications of high-resolution 1H magic-angle
spinning (MAS) solid-state NMR, in particular two-dimensional heteronuclear and …

Cellulose-pectin spatial contacts are inherent to never-dried Arabidopsis primary cell walls: evidence from solid-state nuclear magnetic resonance

T Wang, YB Park, DJ Cosgrove, M Hong - Plant physiology, 2015 - academic.oup.com
The structural role of pectins in plant primary cell walls is not yet well understood because of
the complex and disordered nature of the cell wall polymers. We recently introduced …

Solid‐state NMR spectroscopic methods in chemistry

DD Laws, HML Bitter, A Jerschow - Angewandte Chemie …, 2002 - Wiley Online Library
Over the last decades, NMR spectroscopy has grown into an indispensable tool for chemical
analysis, structure determination, and the study of dynamics in organic, inorganic, and …

SPINEVOLUTION: a powerful tool for the simulation of solid and liquid state NMR experiments

M Veshtort, RG Griffin - Journal of Magnetic Resonance, 2006 - Elsevier
Exact numerical simulations of NMR experiments are often required for the development of
new techniques and for the extraction of structural and dynamic information from the spectra …

Advanced solid-state NMR methods for the elucidation of structure and dynamics of molecular, macromolecular, and supramolecular systems

SP Brown, HW Spiess - Chemical reviews, 2001 - ACS Publications
In polymer science today, much interest is focused on the controlled design of well-ordered
superstructures based on the self-assembly of carefully chosen building blocks. Of particular …

Tackling the defect conundrum in UiO-66: a mixed-linker approach to engineering missing linker defects

B Bueken, N Van Velthoven, A Krajnc… - Chemistry of …, 2017 - ACS Publications
Over the past decade, the zirconium-terephthalate UiO-66 has evolved into one of the most
intensely studied metal–organic frameworks (MOFs) to date. Among the most fascinating …

Acid properties of solid acid catalysts characterized by solid-state 31P NMR of adsorbed phosphorous probe molecules

A Zheng, SJ Huang, SB Liu, F Deng - Physical Chemistry Chemical …, 2011 - pubs.rsc.org
A brief review is presented on acidity characterization of solid acid catalysts by means of
solid-state phosphor-31 magic-angle-spinning nuclear magnetic resonance (31P MAS …

Three structural roles for water in bone observed by solid-state NMR

EE Wilson, A Awonusi, MD Morris, DH Kohn… - Biophysical journal, 2006 - cell.com
Hydrogen-bearing species in the bone mineral environment were investigated using solid-
state NMR spectroscopy of powdered bone, deproteinated bone, and B-type carbonated …

Fluorinated reduced graphene oxide as an interlayer in Li–S batteries

A Vizintin, M Lozinšek, RK Chellappan… - Chemistry of …, 2015 - ACS Publications
We report on the synthesis of fluorinated reduced graphene oxide (F-rGO) by a direct
fluorination of reduced graphene oxide (rGO) with F2 or XeF2/BF3 in anhydrous HF …