Methodological developments for metabolic NMR spectroscopy from cultured cells to tissue extracts: Achievements, progress and pitfalls

NW Lutz, M Bernard - Molecules, 2022 - mdpi.com
This is a broad overview and critical review of a particular group of closely related ex vivo
and in vitro metabolic NMR spectroscopic methods. The scope of interest comprises studies …

StereoPHIP: Stereoselective Parahydrogen‐Induced Polarization

MT Huynh, E Buchanan, S Chirayil… - Angewandte Chemie …, 2023 - Wiley Online Library
Parahydrogen‐induced polarization (PHIP) followed by polarization transfer to 13C is a
rapidly developing technique for the generation of 13C‐hyperpolarized substrates. Chirality …

Design, Synthesis, and Assessment of Tricarboxylic Acid Cycle Probes

J Chen, D Chao, UP Tran, KL Billingsley - Synthesis, 2024 - thieme-connect.com
Hyperpolarized 13 C magnetic resonance spectroscopy can provide unique insights into
metabolic activity in vivo. Despite the advantages of this technology, certain metabolic …

Technical considerations of MRI methods for validating DNP probes in small animals

CE Harrison, J Chen, SH Lin, JM Park - Advances in Magnetic Resonance …, 2024 - Elsevier
Probes that are developed for dissolution dynamic nuclear polarization (DNP) should meet
numerous requirements such as solubility, glassing, and spin-lattice relation time, yet only a …

Beyond 13C-pyruvate: Prospects for biomedical applications of alternative hyperpolarized probes and isotopes

M Mishkovsky, HAI Yoshihara - Advances in Magnetic Resonance …, 2024 - Elsevier
The past 2 decades have witnessed an extensive development of nuclear spin
hyperpolarization technologies. The capability to produce solutions of hyperpolarized …

Hyperpolarized tracer design, synthesis, and characterization

EH Suh, R Eskandari, MT Huynh, G Sharma… - Advances in Magnetic …, 2024 - Elsevier
While NMR offers valuable chemical information, its sensitivity is inherently limited. The
utilization of hyperpolarized NMR techniques, however, can produce significantly enhanced …

[引用][C] The Chemistry of Hyperpolarized Magnetic Resonance Probes

EH Suh, Z Kovacs - 2024 - Academic Press