Electron spin resonance in studies of membranes and proteins

PP Borbat, AJ Costa-Filho, KA Earle, JK Moscicki… - Science, 2001 - science.org
We provide a review of current electron spin resonance (ESR) techniques for studying basic
molecular mechanisms in membranes and proteins by using nitroxide spin labels. In …

New technologies in electron spin resonance

JH Freed - Annual review of physical chemistry, 2000 - annualreviews.org
New electron spin resonance (ESR) technologies have been developed, which have led to
new and improved applications.(a) The development of two-dimensional Fourier transform …

Neutron scattering studies of the model glass former ortho-terphenyl

A Tölle - Reports on Progress in Physics, 2001 - iopscience.iop.org
The van der Waals liquid ortho-terphenyl has long been used as a model system in the
study of the glass transition. Motivated by mode-coupling theory, extensive experiments …

Relaxation times of organic radicals and transition metal ions

SS Eaton, GR Eaton - Distance measurements in biological systems by …, 2000 - Springer
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Solid-state dynamic nuclear polarization at 9.4 and 18.8 T from 100 K to room temperature

M Lelli, SR Chaudhari, D Gajan… - Journal of the …, 2015 - ACS Publications
Efficient dynamic nuclear polarization (DNP) in solids, which enables very high sensitivity
NMR experiments, is currently limited to temperatures of around 100 K and below. Here we …

An assessment of the applicability of multifrequency ESR to study the complex dynamics of biomolecules

Z Liang, JH Freed - The Journal of Physical Chemistry B, 1999 - ACS Publications
It is shown that the commonly used models for analyzing ESR spectra from nitroxide spin-
labeled proteins or DNA systems are special cases of the more general slowly relaxing local …

A multifrequency electron spin resonance study of T4 lysozyme dynamics

JP Barnes, Z Liang, HS Mchaourab, JH Freed… - Biophysical journal, 1999 - cell.com
Electron spin resonance (ESR) spectroscopy at 250GHz and 9GHz is utilized to study the
dynamics and local structural ordering of a nitroxide-labeled enzyme, T4 lysozyme (EC 3.2 …

Dynamical decoupling of nitroxides in o-terphenyl: a study of temperature, deuteration and concentration effects

J Soetbeer, M Hülsmann, A Godt, Y Polyhach… - Physical Chemistry …, 2018 - pubs.rsc.org
We have characterized the temperature dependent transverse relaxation for 100 μM
protonated and deuterated nitroxides in both protonated and deuterated o-terphenyl (OTP …

Hydration, structure, and molecular interactions in the headgroup region of dioleoylphosphatidylcholine bilayers: an electron spin resonance study

M Ge, JH Freed - Biophysical Journal, 2003 - cell.com
The relationship between bilayer hydration and the dynamic structure of headgroups and
interbilayer water in multilamellar vesicles is investigated by electron spin resonance …

Oxygen-17 dynamic nuclear polarisation enhanced solid-state NMR spectroscopy at 18.8 T

NJ Brownbill, D Gajan, A Lesage, L Emsley… - Chemical …, 2017 - pubs.rsc.org
We report 17O dynamic nuclear polarisation (DNP) enhanced solid-state NMR experiments
at 18.8 T. Several formulations were investigated on the Mg (OH) 2 compound. A signal …