Determination of residual fipronil and its metabolites in food samples: A review

X Li, W Ma, H Li, Q Zhang, Z Ma - Trends in Food Science & Technology, 2020 - Elsevier
Background Fipronil is an effective phenylpyrazole insecticide commonly used in agriculture
for pest control. In creature, fipronil could be metabolized to several more toxic metabolites …

The QuEChERS approach for the determination of pesticide residues in soil samples: An overview

K Pszczolińska, M Michel - Journal of AOAC International, 2016 - academic.oup.com
Soil samples are complex matrixes; therefore, soil sample preparation is a critical step, and
one that is usually expensive, time-consuming, and labor intensive. The quick, easy, cheap …

Determination and dissipation of fipronil and its metabolites in peanut and soil

M Li, P Li, L Wang, M Feng, L Han - Journal of agricultural and …, 2015 - ACS Publications
In this study, a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method
was established for the extraction and cleanup of fipronil and its three metabolites (fipronil …

Simultaneous determination and risk assessment of fipronil and its metabolites in sugarcane, using GC-ECD and confirmation by GC-MS/MS

S Biswas, R Mondal, A Mukherjee, M Sarkar, RK Kole - Food chemistry, 2019 - Elsevier
A sensitive gas chromatographic method using a modified QuEChERS technique is reported
for simultaneous determination, dissipation and risk assessment of fipronil and its …

Determination of residual fipronil in chicken egg and muscle by LC–MS/MS

M Zhang, K Bian, T Zhou, X Song, Q Liu… - … of Chromatography B, 2016 - Elsevier
A simple, sensitive and reliable method was developed and applied to the residue analysis
of fipronil in chicken egg and muscle by liquid chromatography-tandem mass spectrometry …

Quenched electrochemiluminescence sensor of ZnO@ g-C3N4 modified glassy carbon electrode for fipronil determination

J Yin, X Chen, Z Chen - Microchemical Journal, 2019 - Elsevier
In this study, a novel quenched electrochemiluminscence (ECL) sensor was constructed
based on the integration of ZnO and gC 3 N 4 for determination of fipronil. The ZnO@ gC 3 N …

Development of a vortex-assisted dispersive liquid-liquid microextraction (VA-DLLME) and LC-MS/MS procedure for simultaneous determination of fipronil and its …

OI Abdallah, NS Ahmed - Food Analytical Methods, 2019 - Springer
A rapid, simple, inexpensive, and reliable vortex-assisted dispersive liquid-liquid
microextraction (VA-DLLME) method was developed for the determination of fipronil and its …

[HTML][HTML] Residue analysis and persistence evaluation of fipronil and its metabolites in cotton using high-performance liquid chromatography-tandem mass …

X Wu, Y Yu, J Xu, F Dong, X Liu, P Du, D Wei… - PLoS One, 2017 - journals.plos.org
A simple residue analytical method based on the QuEChERS approach and high-
performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) detection …

Fipronil residues and risk assessment of Chinese marketed fruits and vegetables: A long-term investigation over 6 years

S Liang, Z Zhao, C Fan, J Xu, H Li, Q Chang, G Pang - Food Control, 2019 - Elsevier
The presence and risk of pesticide residues in fruits and vegetables have been concerned
by the general public. Fipronil has been listed as a banned pesticide in China since 2009 …

Simultaneous determination of three pesticides and their metabolites in unprocessed foods using ultraperformance liquid chromatography-tandem mass spectrometry

L Rong, X Wu, J Xu, F Dong, X Liu, X Pan… - Food Additives & …, 2018 - Taylor & Francis
We have developed a rapid, multi-compound analytical method for measuring residues of
the pesticides thiamethoxam and its metabolite, clothianidin; fipronil and its three …