An overview of the Kjeldahl method of nitrogen determination. Part II. Sample preparation, working scale, instrumental finish, and quality control

P Sáez-Plaza, MJ Navas, S Wybraniec… - Critical Reviews in …, 2013 - Taylor & Francis
The Kjeldahl method was introduced in 1883 and consists of three main steps: sample
digestion, distillation, and ammonia determination (titration being the primary method). The …

Practical guidelines for reporting results in single-and multi-component analytical calibration: A tutorial

AC Olivieri - Analytica Chimica Acta, 2015 - Elsevier
Practical guidelines for reporting analytical calibration results are provided. General topics,
such as the number of reported significant figures and the optimization of analytical …

A practical guide to analytical method validation, including measurement uncertainty and accuracy profiles

AG González, MÁ Herrador - TrAC Trends in Analytical Chemistry, 2007 - Elsevier
The objective of analytical method validation is to ensure that every future measurement in
routine analysis will be close enough to the unknown true value for the content of the analyte …

Fluorescence paper-based sensor for visual detection of carbamate pesticides in food based on CdTe quantum dot and nano ZnTPyP

H Chen, O Hu, Y Fan, L Xu, L Zhang, W Lan, Y Hu… - Food chemistry, 2020 - Elsevier
The needing of rapid and sensitive detection method for pesticides is increasing, to facilitate
its detection without complicated instruments. Herein, a novel paper-based senor was …

[PDF][PDF] Validação de métodos analíticos: estratégia e discussão

NM Brito, OPA Junior, L Polese… - Pesticidas: r. ecotoxicol. e …, 2003 - core.ac.uk
Neste trabalho são apresentadas as definições dos parâmetros (seletividade, limites de
detecção e quantificação, exatidão, precisão, linearidade, gráfico analítico, sensibilidade e …

A novel workflow for semi-quantification of emerging contaminants in environmental samples analyzed by LC-HRMS

R Aalizadeh, V Nikolopoulou, N Alygizakis… - Analytical and …, 2022 - Springer
There is an increasing need for developing a strategy to quantify the newly identified
substances in environmental samples, where there are not always reference standards …

Graphene quantum dots-silver nanoparticles as a novel sensitive and selective luminescence probe for the detection of glyphosate in food samples

J Jiménez-López, EJ Llorent-Martínez… - Talanta, 2020 - Elsevier
Glyphosate (Gly) is the most widely used herbicide at the moment. It presents a broad
spectrum of action, hence its use for many different crops. Regulatory agencies have …

MVC1: an integrated MatLab toolbox for first-order multivariate calibration

AC Olivieri, HC Goicoechea, FA Iñón - Chemometrics and Intelligent …, 2004 - Elsevier
Multivariate calibration 1 (MVC1), a MatLab® toolbox for implementing up to 12 different first-
order calibration methodologies through easily managed graphical user interfaces, is …

Intra-laboratory assessment of method accuracy (trueness and precision) by using validation standards

AG González, MÁ Herrador, AG Asuero - Talanta, 2010 - Elsevier
Assessment of accuracy of analytical methods is a fundamental stage in method validation.
The use of validation standards enables the assessment of both trueness and precision of …

Fabrication of a novel enzymatic electrochemical biosensor for determination of tyrosine in some food samples

K Varmira, G Mohammadi, M Mahmoudi… - Talanta, 2018 - Elsevier
In this work, fabrication of a novel and ultrasensitive electrochemical biosensor based on
immobilization of tyrosine hydroxylase onto palladium-platinum bimetallic alloy …