[图书][B] Two-dimensional NMR spectroscopy: applications for chemists and biochemists

WR Croasmun, RMK Carlson - 1996 - books.google.com
This volume covers the new methodological advances in NMR spectroscopy that have been
developed since the publication of the first edition. These include:'indirect …

Modified BIRD pulses and design of heteronuclear pulse sequences

D Uhrin, T Liptaj, KE Kover - Journal of Magnetic Resonance, Series A, 1993 - Elsevier
A simple modification of BIRD pulses, which removes the inversion effect on an X nucleus
and retains a chemical-shift evolution of the heterospin, is proposed. This modification …

Constituents of the Roots and Leaves of Ekebergia capensis and Their Potential Antiplasmodial and Cytotoxic Activities

BN Irungu, JA Orwa, A Gruhonjic, PA Fitzpatrick… - Molecules, 2014 - mdpi.com
A new triterpenoid, 3-oxo-12β-hydroxy-oleanan-28, 13β-olide (1), and six known
triterpenoids 2–7 were isolated from the root bark of Ekebergia capensis, an African …

Diosgenin-bearing, molluscicidal saponins from Allium vineale: an NMR approach for the structural assignment of oligosaccharide units

S Chen, JK Snyder - The Journal of Organic Chemistry, 1989 - ACS Publications
An investigation into the molluscicidal substituents of field garlic, Allium vineale, has resulted
in the isolation and identification of seven new saponins with up to six sugars. The isolations …

[PDF][PDF] Improved performance accordion heteronuclear multiple-bond correlation spectroscopy—IMPEACH-MBC

CE Hadden, GE Martin… - Journal of Magnetic …, 1999 - academia.edu
A modification of the recently reported ACCORD-HMBC longrange heteronuclear shift
correlation experiment is described. The new experiment, IMPEACH-MBC (improved …

Cytotoxic Quinones from the Roots of Aloe dawei

N Abdissa, M Induli, P Fitzpatrick, JP Alao… - Molecules, 2014 - mdpi.com
Seven naphthoquinones and nine anthraquinones were isolated from the roots of Aloe
dawei by chromatographic separation. The purified metabolites were identified by NMR and …

Artifacts in two-dimensional NMR

AD Bain, IW Burton, WF Reynolds - Progress in nuclear magnetic …, 1994 - Elsevier
An artifact, as the word is often used in the context of pulse and two-dimensional NMR,“)
refers to an unexpected peak or distortion in the spectrum. In an experimental science, these …

Insight into β-hairpin stability: a structural and thermodynamic study of diastereomeric β-hairpin mimetics

M Erdélyi, V Langer, A Karlén, A Gogoll - New Journal of Chemistry, 2002 - pubs.rsc.org
Two diastereomers of a model β-hairpin peptide mimetic were synthesized and studied with
a combination of experimental (NMR, X-ray, CD, MS, IR) and computational methods (Monte …

Clavudiol A and clavirolide A, two marine dolabellane diterpenes from the soft coral Clavularia viridis

J Su, Y Zhong, K Shi, Q Cheng, JK Snyder… - The Journal of …, 1991 - ACS Publications
The structures of two new marine diterpenes, clavudiol A (1) and clavirolide A (2), isolated
from the Pacific soft coral Clavularia viridis collected off the Xisha Islands in the South China …

Busseihydroquinones A–D from the Roots of Pentas bussei

M Endale, A Ekberg, HM Akala, JP Alao… - Journal of Natural …, 2012 - ACS Publications
Four new naphthohydroquinones, named busseihydroquinones A–D (1–4), along with a
known homoprenylated dihydronaphthoquinone (5), were isolated from the CH2Cl2/MeOH …