[HTML][HTML] Pure shift NMR

K Zangger - Progress in nuclear magnetic resonance spectroscopy, 2015 - Elsevier
Although scalar-coupling provides important structural information, the resulting signal
splittings significantly reduce the resolution of NMR spectra. Limited resolution is a particular …

Broadband 1H homodecoupled NMR experiments: recent developments, methods and applications

L Castañar, T Parella - Magnetic Resonance in Chemistry, 2015 - Wiley Online Library
In recent years, a great interest in the development of new broadband 1H homonuclear
decoupled techniques providing simplified JHH multiplet patterns has emerged again in the …

[HTML][HTML] Spatial encoding and spatial selection methods in high-resolution NMR spectroscopy

JN Dumez - Progress in nuclear magnetic resonance spectroscopy, 2018 - Elsevier
A family of high-resolution NMR methods share the common concept of acquiring in parallel
different sub-experiments in different spatial regions of the NMR tube. These spatial …

[HTML][HTML] Faster and cleaner real-time pure shift NMR experiments

J Mauhart, S Glanzer, P Sakhaii, W Bermel… - Journal of Magnetic …, 2015 - Elsevier
Real-time pure shift experiments provide highly resolved proton NMR spectra which do not
require any special processing. Although being more sensitive than their pseudo 2D …

The impact of the ionic cross-linking mode on the physical and in vitro dexamethasone release properties of chitosan/hydroxyapatite beads

MJ L. Dantas, BF F. dos Santos, A A. Tavares… - Molecules, 2019 - mdpi.com
In this study, the effect of the ionic cross-linking mode on the ability to control physical
properties and in vitro release behavior of the dexamethasone (DEX) drug from chitosan …

Clean G-SERF an NMR experiment for the complete eradication of axial peaks and undesired couplings from the complex spectrum

SK Mishra, N Lokesh, N Suryaprakash - RSC advances, 2017 - pubs.rsc.org
The G-SERF and other related experiments are very useful in the measurement of proton–
proton couplings from the overlapped spectrum. However, they suffer from the presence of …

Minimising research bottlenecks by decluttering NMR spectra

JA Aguilar, J Cassani, M Delbianco… - … A European Journal, 2015 - Wiley Online Library
The lack of resolving power in everyday NMR produces ambiguous data, causing
bottlenecks, lengthening multi‐step projects and increasing the likelihood of making …

A quarter of a century of SERF: The progress of an NMR pulse sequence and its application

S Berger - Progress in Nuclear Magnetic Resonance …, 2018 - Elsevier
SERF, an NMR pulse sequence for selectively measuring a spin coupling constant without
interference from other couplings, was published by the current author almost 25 years ago …

A pure shift experiment with increased sensitivity and superior performance for strongly coupled systems

J Ilgen, L Kaltschnee, CM Thiele - Journal of Magnetic Resonance, 2018 - Elsevier
Motivated by the persisting need for enhanced resolution in solution state NMR spectra,
pure shift techniques such as Zangger-Sterk decoupling have recently attracted widespread …

Accurate measurement of JHH in overlapped signals by a TOCSY‐edited SERF Experiment

A Fredi, P Nolis, T Parella - Magnetic Resonance in Chemistry, 2017 - Wiley Online Library
Selective refocusing (GSERF or the recent PSYCHEDELIC) experiments were originally
designed to determine all proton–proton coupling constants (JHH) for a selected proton …