Chemical equipment has to form a robust and efficient process space and was developed
over the last centuries to very sophisticated, often highly specialized devices. With the …

We report an isothermal flow calorimeter for characterization of reaction enthalpy and
kinetics. The platform consists of a thermoelectric element and a glass–silicon microreactor …

Calorimetric data from chemical reactions such as reaction enthalpy, adiabatic temperature
rise, and activation energy are essential for reaction safety and scale-up from laboratory …

A safe and scalable synthesis of diaryliodonium triflates was achieved using a practical
continuous-flow design. A wide array of electron-rich to electron-deficient arenes could …

Continuous manufacturing and development of flow processes depend significantly on an
optimized and adapted determination of thermokinetic data of chemical reactions. Reaction …

A new method for the calorimetric characterization of high-energetic, fast reactions in flow
mode was developed. The use of an engineered flow reactor in combination with a process …

In this paper, a microsystem integrated with infrared thermography is developed to measure
the kinetics of fast exothermic reactions. The hydrolysis of ethyl acetate is chosen as the …

A key parameter for reactor design and safety evaluation is the reaction enthalpy (ΔHr).
Flash chemistry is a field of chemical synthesis where fast reactions are performed in a …

A flexible reactor and measurement setup to safely obtain thermokinetic data for exothermic
chemical reactions in plate‐type microreactors is presented. Precise heat flux measurement …

Reaction calorimetry of flow processes is important for scale-up and safety in flow chemistry.
Due to the increasing number of flow processes, corresponding flow calorimeters are …