1H-Detected Biomolecular NMR under Fast Magic-Angle Spinning

T Le Marchand, T Schubeis, M Bonaccorsi… - Chemical …, 2022 - ACS Publications
Since the first pioneering studies on small deuterated peptides dating more than 20 years
ago, 1H detection has evolved into the most efficient approach for investigation of …

Solid-state NMR: Methods for biological solids

S Ahlawat, KR Mote, NA Lakomek… - Chemical Reviews, 2022 - ACS Publications
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …

Cellulose-pectin spatial contacts are inherent to never-dried Arabidopsis primary cell walls: evidence from solid-state nuclear magnetic resonance

T Wang, YB Park, DJ Cosgrove, M Hong - Plant physiology, 2015 - academic.oup.com
The structural role of pectins in plant primary cell walls is not yet well understood because of
the complex and disordered nature of the cell wall polymers. We recently introduced …

Structure and interactions of plant cell-wall polysaccharides by two-and three-dimensional magic-angle-spinning solid-state NMR

M Pérez García, Y Zhang, J Hayes, A Salazar… - Biochemistry, 2011 - ACS Publications
The polysaccharide-rich cell walls (CWs) of plants perform essential functions such as
maintaining tensile strength and allowing plant growth. Using two-and three-dimensional …

Spinning faster: protein NMR at MAS frequencies up to 126 kHz

S Penzel, A Oss, ML Org, A Samoson… - Journal of biomolecular …, 2019 - Springer
We report linewidth and proton T 1, T 1 ρ and T 2′ relaxation data of the model protein
ubiquitin acquired at MAS frequencies up to 126 kHz. We find a predominantly linear …

Molecular architecture of chitin and chitosan-dominated cell walls in zygomycetous fungal pathogens by solid-state NMR

Q Cheng, MC Dickwella Widanage, JR Yarava… - Nature …, 2024 - nature.com
Zygomycetous fungal infections pose an emerging medical threat among individuals with
compromised immunity and metabolic abnormalities. Our pathophysiological understanding …

UV pretreatment impairs the enzymatic degradation of polyethylene terephthalate

P Falkenstein, D Gräsing, P Bielytskyi… - Frontiers in …, 2020 - frontiersin.org
The biocatalytic degradation of polyethylene terephthalate (PET) emerged recently as a
promising alternative plastic recycling method. However, limited activity of previously known …

Quantitative analysis of protein backbone dynamics in microcrystalline ubiquitin by solid-state NMR spectroscopy

P Schanda, BH Meier, M Ernst - Journal of the American Chemical …, 2010 - ACS Publications
Characterization of protein dynamics by solid-state NMR spectroscopy requires robust and
accurate measurement protocols, which are not yet fully developed. In this study, we …

PISEMA solid-state NMR spectroscopy

A Ramamoorthy, Y Wei, DK Lee - Annual reports on NMR spectroscopy, 2004 - Elsevier
Gone are the days when solid-state NMR spectroscopy was considered to be untouchable-
like as it provided unappealing spectral lines due to poor resolution and sensitivity …

Membrane Protein Topology Probed by 1H Spin Diffusion from Lipids Using Solid-State NMR Spectroscopy

D Huster, X Yao, M Hong - Journal of the American Chemical …, 2002 - ACS Publications
We describe a two-dimensional solid-state NMR technique to investigate membrane protein
topology under magic-angle spinning conditions. The experiment detects the rate of 1H spin …