Natural Abundance 17O DNP Two-Dimensional and Surface-Enhanced NMR Spectroscopy

FA Perras, T Kobayashi, M Pruski - Journal of the American …, 2015 - ACS Publications
Due to its extremely low natural abundance and quadrupolar nature, the 17O nuclide is very
rarely used for spectroscopic investigation of solids by NMR without isotope enrichment …

Detection of remote proton–nitrogen correlations by 1 H-detected 14 N overtone solid-state NMR at fast MAS

NT Duong, Y Nishiyama - Physical Chemistry Chemical Physics, 2022 - pubs.rsc.org
Detecting proton and nitrogen correlations in solid-state nuclear magnetic resonance (NMR)
is important for the structural determination of biological and chemical systems. Recent …

Fast Magic-Angle Spinning Three-Dimensional NMR Experiment for Simultaneously Probing H H and N H Proximities in Solids

GNM Reddy, M Malon, A Marsh, Y Nishiyama… - Analytical …, 2016 - ACS Publications
A fast magic-angle spinning (MAS, 70 kHz) solid-state NMR experiment is presented that
combines 1H Double-Quantum (DQ) and 14N 1H HMQC (Heteronuclear Multiple …

[HTML][HTML] Fokker-Planck formalism in magnetic resonance simulations

I Kuprov - Journal of magnetic resonance, 2016 - Elsevier
This paper presents an overview of the Fokker-Planck formalism for non-biological magnetic
resonance simulations, describes its existing applications and proposes some novel ones …

Recent advances in 14N solid-state NMR

E Dib, T Mineva, B Alonso - Annual Reports on NMR Spectroscopy, 2016 - Elsevier
This chapter is devoted to the recent advances in 14 N solid-state NMR related to both
theoretical and practical aspects. First, the last NMR methods developed to facilitate the …

Solid-state NMR of nanocrystals

T Gutmann, PB Groszewicz, G Buntkowsky - Annual Reports on NMR …, 2019 - Elsevier
Recent advances in solid-state nuclear magnetic resonance (NMR) spectroscopy and
dynamic nuclear polarization (DNP) of nanostructured materials are reviewed. A first group …

Time domain simulation of Gd3+–Gd3+ distance measurements by EPR

N Manukovsky, A Feintuch, I Kuprov… - The Journal of chemical …, 2017 - pubs.aip.org
Gd 3+-based spin labels are useful as an alternative to nitroxides for intramolecular distance
measurements at high fields in biological systems. However, double electron-electron …

Selective 1H-14N Distance Measurements by 14N Overtone Solid-State NMR Spectroscopy at Fast MAS

NT Duong, Z Gan, Y Nishiyama - Frontiers in Molecular Biosciences, 2021 - frontiersin.org
Accurate distance measurements between proton and nitrogen can provide detailed
information on the structures and dynamics of various molecules. The combination of …

Double cross polarization for the indirect detection of nitrogen-14 nuclei in magic angle spinning NMR spectroscopy

D Carnevale, X Ji, G Bodenhausen - The Journal of Chemical Physics, 2017 - pubs.aip.org
Nitrogen-14 NMR spectra at fast magic-angle spinning rates can be acquired indirectly by
means of two-dimensional techniques based on double cross polarization transfer 1 H→ 14 …

PRESTO polarization transfer to quadrupolar nuclei: implications for dynamic nuclear polarization

FA Perras, T Kobayashi, M Pruski - Physical Chemistry Chemical …, 2015 - pubs.rsc.org
We show both experimentally and numerically on a series of model systems that in
experiments involving transfer of magnetization from 1H to the quadrupolar nuclei under …